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Yüzeyi ZnO Nanopartikülleri ile Kaplanmış Demir Matrisli Malzemelerin Karakterizasyonu ve Mekanik Özelliklerinin İncelenmesi

Year 2020, Volume: 8 Issue: 2, 365 - 370, 26.05.2020
https://doi.org/10.21541/apjes.658644

Abstract

Bu çalışmanın amacı toz metalürjisi ile demir ve demir-karbon alaşım malzemelerinin üretilmesi ve bu malzemelerin çinko oksit (ZnO) ile kaplanmasıyla mekanik özelliklerdeki artışı ortaya çıkarmaktır. Bu amaçla, demir ve demir-karbon alaşımı malzemeler toz metalürjisi ile üretilmiştir. Karbon malzeme olarak, aktif karbon, grafit, grafen, karbon nanotüp, vb. gibi yaygın kullanılan karbon malzemelere alternatif olabilecek, glukozdan sentezlenen hidrotermal karbonlar kullanılmıştır. Karbonlu ve karbonsuz demir malzemelerin yüzeyi SILAR metoduyla yaklaşık 200±17 nm uzunluğundaki çinko oksit partikülleri tarafından kaplanmıştır. Bu kompozitlerin yapısı SEM, SEM-EDX ve XRD analizleri ile karakterize edilmiştir. Malzemelerin mekanik özelliklerine ZnO kaplamanın etkisi ise sertlik ve korozyon testleri ile incelenmiştir. Bu sonuçlara göre, ZnO kaplanmış kompozitlerin hem sertlik değerlerinde (%44 ve %73) hem de korozyon dayanımlarında (%118 ve %60) kaplamasız malzemelere kıyasla önemli derece artış meydana gelmiştir.

References

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Year 2020, Volume: 8 Issue: 2, 365 - 370, 26.05.2020
https://doi.org/10.21541/apjes.658644

Abstract

References

  • [1] L. Zhong, Y. Xu, M. Hojamberdiev, J. Wang, ve J. Wang, “In situ fabrication of titanium carbide particulates-reinforced iron matrix composites”, Materials & design, c. 32, sy 7, ss. 3790–3795, 2011.
  • [2] X. Zhang, F. Ma, K. Ma, ve X. Li, “Effects of graphite content and temperature on microstructure and mechanical properties of Iron-based powder metallurgy parts”, Journal of Materials Science Research, c. 1, sy 4, s. 48, 2012.
  • [3] M. A. Erden, S. Gündüz, M. Türkmen, ve H. Karabulut, “Microstructural characterization and mechanical properties of microalloyed powder metallurgy steels”, Materials Science and Engineering: A, c. 616, ss. 201–206, 2014.
  • [4] M. Türkmen, H. Karabulut, M. A. Erden, ve S. Gündüz, “EFFECT OF TIN ADDITION ON THE MICROSTRUCTURE AND MECHANICAL PROPERTIES OF PM STEELS”, Technological Applied Sciences, c. 12, sy 4, ss. 178–184.
  • [5] C. Krishnamurthy Srinivasa, C. Suryanarayana Ramesh, ve S. K. Prabhakar, “Blending of iron and silicon carbide powders for producing metal matrix composites by laser sintering process”, Rapid Prototyping Journal, c. 16, sy 4, ss. 258–267, 2010.
  • [6] P. Gupta, D. Kumar, M. A. Quraishi, ve O. Parkash, “Corrosion behavior of Al2O3 reinforced Fe metal matrix nanocomposites produced by powder metallurgy technique”, Advanced Science, Engineering and Medicine, c. 5, sy 4, ss. 366–370, 2013.
  • [7] L. Xie, X. Xiong, Y. Zeng, ve Y. Wang, “The wear properties and mechanism of detonation sprayed iron-based amorphous coating”, Surface and Coatings Technology, c. 366, ss. 146–155, 2019.
  • [8] S. Shi, Y. Zhao, Z. Zhang, ve L. Yu, “Corrosion protection of a novel SiO2@ PANI coating for Q235 carbon steel”, Progress in Organic Coatings, c. 132, ss. 227–234, 2019.
  • [9] D. Kallappa ve V. T. Venkatarangaiah, “Synthesis of CeO2 doped ZnO nanoparticles and their application in Zn-composite coating on mild steel”, Arabian Journal of Chemistry, 2018.
  • [10] L. Exbrayat vd., “Electrodeposition of zinc–ceria nanocomposite coatings in alkaline bath”, Journal of Solid State Electrochemistry, c. 18, sy 1, ss. 223–233, 2014.
  • [11] A. Mahmood ve A. Naeem, “Sol-Gel-Derived Doped ZnO Thin Films: Processing, Properties, and Applications”, Recent Applications in Sol-Gel Synthesis, ss. 169–193, 2017.
  • [12] L. Znaidi, “Sol–gel-deposited ZnO thin films: A review”, Materials Science and Engineering: B, c. 174, sy 1-3, ss. 18–30, 2010.
  • [13] C. Duman ve H. Guney, “Influence of annealing and optical aging on optical and structural properties of ZnO thin films obtained by SILAR method”, Lithuanian Journal of Physics, c. 57, sy 4, 2017.
  • [14] A. Raidou vd., “Characterization of ZnO thin films grown by SILAR method”, Open Access Library Journal, c. 1, sy 3, 2014.
  • [15] H. Simsir, N. Eltugral, ve S. Karagoz, “Hydrothermal carbonization for the preparation of hydrochars from glucose, cellulose, chitin, chitosan and wood chips via low-temperature and their characterization”, Bioresource technology, c. 246, ss. 82–87, 2017.
  • [16] M.-M. Titirici, R. J. White, C. Falco, ve M. Sevilla, “Black perspectives for a green future: hydrothermal carbons for environment protection and energy storage”, Energy & Environmental Science, c. 5, sy 5, ss. 6796–6822, 2012.
  • [17] P.-Y. Lee, S.-P. Chang, ve S.-J. Chang, “Synthesis and optical properties of ZnO thin films prepared by SILAR method with ethylene glycol”, Advances in nano research, c. 1, sy 2, ss. 93–103, 2013.
  • [18] W.-S. Lin, H.-M. Lin, H.-H. Chen, Y.-K. Hwu, ve Y.-J. Chiou, “Shape effects of iron nanowires on hyperthermia treatment”, Journal of Nanomaterials, c. 2013, s. 9, 2013.
  • [19] E. Otero, A. Pardo, M. V. Utrilla, E. Saenz, ve J. F. Alvarez, “Corrosion behaviour of AISI 304L and 316L stainless steels prepared by powder metallurgy in the presence of sulphuric and phosphoric acid”, Corrosion Science, c. 40, sy 8, ss. 1421–1434, 1998.
  • [20] Y.-S. Kim ve J.-G. Kim, “Corrosion behavior of pipeline carbon steel under different iron oxide deposits in the district heating system”, Metals, c. 7, sy 5, s. 182, 2017.
  • [21] Y. Y. Li, Z. Z. Wang, X. P. Guo, ve G. A. Zhang, “Galvanic corrosion between N80 carbon steel and 13Cr stainless steel under supercritical CO2 conditions”, Corrosion Science, c. 147, ss. 260–272, 2019.
There are 21 citations in total.

Details

Primary Language Turkish
Subjects Engineering
Journal Section Articles
Authors

Hamza Şimşir 0000-0002-6794-1046

Publication Date May 26, 2020
Submission Date December 12, 2019
Published in Issue Year 2020 Volume: 8 Issue: 2

Cite

IEEE H. Şimşir, “Yüzeyi ZnO Nanopartikülleri ile Kaplanmış Demir Matrisli Malzemelerin Karakterizasyonu ve Mekanik Özelliklerinin İncelenmesi”, APJES, vol. 8, no. 2, pp. 365–370, 2020, doi: 10.21541/apjes.658644.