Determination of 12 heavy metals in hennas by microwave induced plasma optical emission spectrometry

Nil Ozbek

doi:10.18596/jotcsa.423820

Research Article

Determination of 12 heavy metals in hennas by microwave induced plasma optical emission spectrometry

Year 2018, , 857 - 868, 01.01.2018

Nil Ozbek

https://doi.org/10.18596/jotcsa.423820

Cited By: 8

Abstract

In this study, Al, B ,Cd, Co, Cr, Cu, Fe, Mn, Mo, Ni, Pb and
Sn concentrations in henna samples sold in
Turkey were determined by Microwave Induced Plasma Optical Emission
Spectrometry. It is a relatively new technique, which uses a 2.45 GHz microwave magnetic field and nitrogen gas to
sustain the plasma. With this technique, there is no requirement for flammable
and toxic gases and their gas-cylinders. For the determination, each henna sample weighed approximately 0.1 g and underwent microwave-assisted
digestion using 10 mL of HNO₃+H₂O₂ (3:1)
mixture. In order to test the method’s accuracy, analytes were determined in bush branches and the leaves CRM. Finally, the elemental
concentrations were determined in 18 different henna samples sold in Turkey by using
optimized parameters.

Keywords

Microwave Induced Plasma Optical Emission Spectrometry, henna, Lawsonia inermis

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